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山核桃油的提取工藝及其特性研究
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    對(duì)乙醚浸提法提取山核桃油的工藝條件進(jìn)行了試驗(yàn)。結(jié)果表明:液料比大于4 mL/g、提取溫度為55~65℃、提取時(shí)間2.5 h,山核桃油的提取率較高。在單因素試驗(yàn)的基礎(chǔ)上用正交試驗(yàn)得出優(yōu)化工藝條件為:液料比為5 mL/g、溫度65℃、時(shí)間2.5 h,在該條件下山核桃油的提取率為98.17%。油脂的理化指標(biāo)為:碘價(jià)92.20 g/100 g、折光指數(shù)n201.471 0、相對(duì)密度d200.905 6、酸價(jià)0.750 mg/g。采用氣相色譜-質(zhì)譜分析儀對(duì)油脂的脂肪酸組成及含量進(jìn)行了測(cè)定,結(jié)果表明,不飽和脂肪酸質(zhì)量分?jǐn)?shù)為91.51%,其中油酸和亞油酸質(zhì)量分?jǐn)?shù)為

    Abstract:

    91.13%。 The ether extracting technology of carya kernel oil was experimentally studied in this work. The result showed that a high extraction rate could be achieved when the ratio of solution/material was higher than 4 mL/g,operating temperatures ranged from 55 to 65℃ and the duration of extraction was 2.5 h. On basis of single factor experiment,the orthogonal trial was used in optimization of technological parameters,the optimum technological condition was 5 mL/g,2.5 h and 65℃,under which the extraction rate could be high as 98.17%. Physicochemical properties of the oil are as follows: the iodine value is 92.20 g/100 g; the refractive index n201.471 0, density d200.905 6 and the acid value 750 mg/g. The unsaturated fatty acid in the oil was 91.51%,the oleic acid and the linoleic acid was both 91.13% determined by the gas chromatography-mass spectroscopy(GC-MS).

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周明亮,王鴻飛,趙丹.山核桃油的提取工藝及其特性研究[J].農(nóng)業(yè)機(jī)械學(xué)報(bào),2007,38(3):95-98.[J]. Transactions of the Chinese Society for Agricultural Machinery,2007,38(3):95-98.

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