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基于SPME-GC-MS的超高壓處理黑莓汁香氣分析
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國(guó)家高技術(shù)研究發(fā)展計(jì)劃(863計(jì)劃)資助項(xiàng)目(2007AA100405)和江蘇高校優(yōu)勢(shì)學(xué)科建設(shè)工程資助項(xiàng)目


Aromatic Compounds in Blackberry Juice after Ultrahigh Pressure Treatment by SPME-GC-MS
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    摘要:

    采用固相微萃取與氣相色譜-質(zhì)譜儀(GC-MS)聯(lián)用檢測(cè),對(duì)超高壓處理前、后黑莓清汁香氣成分進(jìn)行分析和感官評(píng)價(jià)。結(jié)果表明:經(jīng)超高壓處理的黑莓清汁香氣種類與原汁相同,但不同成分的含量略有變化,300 MPa 處理10 min的黑莓清汁醇類、酯類含量減少了4.8%和11.1%,醛類、酮類含量增加了12.06%和14.59%;400 MPa處理10 min后,其內(nèi)的醇類、酯類、醛類含量增加4.9%、26.86%和9.9%;而200、500和600 MPa處理10 min的黑莓清汁醇類、酯類、醛類含量均無顯著變化。感官評(píng)定表明,400 MPa處理10 min能較好地保留黑莓清汁典型濃郁的香氣,且與GC-MS檢測(cè)分析結(jié)果一致。

    Abstract:

    The aromatic compounds in blackberry juice before and after ultrahigh pressure (UHP) treatment were evaluated by sensory evaluation and analyzed by combining SPME with GC-MS method. The results showed that after UHP, the categories of aromatic compounds in blackberry juice were the same as those in original samples, however, the content had a little change after UHP treatment. The alcohols and esters contents were decreased by 4.8% and 11.1% respectively after 300 MPa, 10 min treatment. While the contents of aldehydes and the ketones were respectively increased by 12.06% and 14.59%; and the alcohols, esters and aldehydes contents were increased by 4.9%, 26.86% and 9.9% after 400 MPa,10 min treatment. But the concentrations of them were not changed significantly after 200 MPa, 500 MPa and 600 MPa, 10 min treatment. The sensory evaluation results demonstrate that blackberry juice under 400 MPa, 10 min treatment has its typical flavor, and matches well with the GC-MS analysis results.

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馬永昆,白潔,魏本喜,張龍,馬善麗,蔣家奎.基于SPME-GC-MS的超高壓處理黑莓汁香氣分析[J].農(nóng)業(yè)機(jī)械學(xué)報(bào),2011,42(7):170-175. Ma Yongkun, Bai Jie, Wei Benxi, Zhang Long, Ma Shanli, Jiang Jiakui. Aromatic Compounds in Blackberry Juice after Ultrahigh Pressure Treatment by SPME-GC-MS[J]. Transactions of the Chinese Society for Agricultural Machinery,2011,42(7):170-175.

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