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微波裂解光皮樹(shù)油皂化物脫羧制備烴類燃料研究
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國(guó)家自然科學(xué)基金資助項(xiàng)目(30960304)、國(guó)際科技合作計(jì)劃資助項(xiàng)目 (2010DFB63750)、江西省科技廳產(chǎn)業(yè)化關(guān)鍵技術(shù)攻關(guān)資助項(xiàng)目(2007BN12100)、國(guó)家林業(yè)局948資助項(xiàng)目（2010409）和江西省國(guó)際合作資助項(xiàng)目(2010EHB03200)


Microwave-assisted Pyrolysis of Swida wilsonianaFruit Oil Soap for Preparing Renewable Hydrocarbon Fuel via Selective Decarboxylation
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    摘要:

    以光皮樹(shù)果實(shí)油脂通過(guò)皂化反應(yīng)獲得的皂類為研究對(duì)象，利用微波裂解選擇性加熱優(yōu)勢(shì)開(kāi)展皂類脫羧制備烴類燃料研究。通過(guò)氣質(zhì)聯(lián)用等方法對(duì)裂解產(chǎn)物的分析表明，單純鈉皂微波裂解所得到液態(tài)產(chǎn)物一般都在皂類干質(zhì)量的70%以上，裂解液態(tài)產(chǎn)物的密度為0.850～0.875g/cm3，運(yùn)動(dòng)粘度為2.09～2.85mm2/s，與柴油的性質(zhì)基本相似。裂解液態(tài)產(chǎn)物中最高峰是十五碳烯，證實(shí)脫羧是皂類微波裂解的主要反應(yīng)形式。

    Abstract:

    In order to prepare hydrocarbon fuel, sodium soap made from Swida wilsoniana fruit oil was chosen as a model compound with significant molecular polarity for preparing hydrocarbon fuel by microwaveassisted pyrolysis. The result showed that the hydrocarbon content were usually above 70%. In addition, its density and dynamic viscosity were 0.850～0.875 /cm3 and 2.09～2.85 mm2/s, respectively, similar with petroleum diesel. The highest peak in the GC-S profile of liquid product was fifteen carbon alkenes, decarboxylation was proved to be main reaction in microwaveassisted pyrolysis.

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劉玉環(huán),王允圃,王應(yīng)寬,萬(wàn)益琴,張錦勝,阮榕生.微波裂解光皮樹(shù)油皂化物脫羧制備烴類燃料研究[J].農(nóng)業(yè)機(jī)械學(xué)報(bào),2012,43(2):106-111,105. Liu Yuhuan, Wang Yunpu, Wang Yingkuan, Wan Yiqin, Zhang Jinsheng, Ruan Rongsheng. Microwave-assisted Pyrolysis of Swida wilsonianaFruit Oil Soap for Preparing Renewable Hydrocarbon Fuel via Selective Decarboxylation[J]. Transactions of the Chinese Society for Agricultural Machinery,2012,43(2):106-111,105.

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  • 在線發(fā)布日期: 2012-02-17
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