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丁香抗氧化活性物質(zhì)超聲波-微波協(xié)同提取技術(shù)
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國家自然科學(xué)基金資助項(xiàng)目(31360371)、江西省自然科學(xué)基金資助項(xiàng)目(20132BAB204030)、江西省教育廳科技資助項(xiàng)目(GJJ12620)、江西省科技支撐計(jì)劃資助項(xiàng)目(20123BBF60150)和江西省衛(wèi)生廳中醫(yī)藥科研計(jì)劃資助項(xiàng)目(2013A017)


Extraction Technology of Antioxidants from Clove Based on Simultaneous Ultrasonic/Microwave Assisted Extraction
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    摘要:

    采用超聲波-微波協(xié)同技術(shù)對丁香抗氧化活性物質(zhì)提取工藝進(jìn)行了優(yōu)化,并對該技術(shù)高效提取機(jī)理進(jìn)行了分析。結(jié)果表明,丁香抗氧化活性物質(zhì)超聲波-微波協(xié)同提取最佳工藝條件為:50%乙醇、液料比30mL/g、超聲波功率50W、微波功率100W、協(xié)同提取時(shí)間12min。通過對比分析發(fā)現(xiàn),超聲波-微波協(xié)同對丁香抗氧化活性物質(zhì)的提取效率顯著高于水浴振蕩提?。≒<0.01);協(xié)同提取技術(shù)優(yōu)勢在于超聲波和微波的協(xié)同作用,實(shí)現(xiàn)優(yōu)勢互補(bǔ),從而對原料細(xì)胞結(jié)構(gòu)破壞更嚴(yán)重,作用更充分,提高了提取效率。

    Abstract:

    The simultaneous ultrasonic/microwave assisted extraction (UMAE) technology of extracting antioxidants from clove was optimized and the reason for high-efficiency of this method was analyzed. The results show that the optimal parameters of the UMAE technology were as follows, ethanol concentration was 50%, ratio of extracting solution to sample was 30mL/g, ultrasonic power was 50W, the microwave power was 100W and the extracting time was 12min. Comparative study show that the extraction ratio of antioxidants from clove by UMAE was significantly improved compared with water bath oscillator extraction (WBOE) in the same conditions. It was also found that the superiority of UMAE was simultaneously acted and mutually reinforced by ultrasonic and microwave through interaction analysis. A comparison of scanning electron microscopy images from the clove powders by UMAE, WBOE, microwave assisted extraction (MAE) and ultrasonic assisted extraction (UAE) indicated the extraction efficiency was higher by UMEA with the more serious disruption of cell structure and the more sufficient interaction.

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劉常金,趙 錦,江慎華,王 煌,廖 亮,張小谷.丁香抗氧化活性物質(zhì)超聲波-微波協(xié)同提取技術(shù)[J].農(nóng)業(yè)機(jī)械學(xué)報(bào),2014,45(11):223-229. Liu Changjin, Zhao Jin, Jiang Shenhua, Wang Huang, Liao Liang, Zhang Xiaogu. Extraction Technology of Antioxidants from Clove Based on Simultaneous Ultrasonic/Microwave Assisted Extraction[J]. Transactions of the Chinese Society for Agricultural Machinery,2014,45(11):223-229.

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  • 收稿日期:2013-11-16
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  • 在線發(fā)布日期: 2014-11-10
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